Dynamic HPLC study of C70 chlorination reveals a surprisingly selective synthesis of C70Cl8

Igor V. Kuvychko; Alexey A. Popov; Alexey V. Streletskii; Leanne C. Nye; Thomas Drewello; Steven H. Strauss; Olga V. Boltalina

doi:10.1039/C0CC03134H

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Chemical Communications

Issue 43, 2010

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Dynamic HPLC study of C₇₀ chlorination reveals a surprisingly selective synthesis of C₇₀Cl₈

Igor V. Kuvychko , Alexey A. Popov , Alexey V. Streletskii , Leanne C. Nye , Thomas Drewello , Steven H. Strauss and Olga V. Boltalina

Chem. Commun., 2010,46, 8204-8206

DOI: 10.1039/C0CC03134H
Received 09 Aug 2010, Accepted 03 Sep 2010
First published on the web 27 Sep 2010
This article is part of the collection: Carbon nanostructures

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Abstract
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A dynamic HPLC study of C₇₀ chlorination led to the discovery, isolation, characterization, and development of the efficient preparatory procedures for two previously unknown soluble chlorofullerenes C₇₀Cl₈ and C₇₀Cl₆ and for insoluble [C₇₀Cl₈]_n. A novel synthesis of 99% pure C₇₀Cl₁₀ with a nearly quantitative yield was also developed. The first stability study of C₇₀Cl_10,8,6 in solution showed that these compounds are very light-sensitive.