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Issue 10, 2008
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An efficient method for synthesising unsymmetrical silaketals: substrates for ring-closing, including macrocycle-closing, metathesis

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Abstract

Diisopropylsilyl ethers were activated with N-bromosuccinimide, and reacted with a fluorous-tagged alcohol, to yield tethered substrates for ring-closing metathesis reactions.

Graphical abstract: An efficient method for synthesising unsymmetrical silaketals: substrates for ring-closing, including macrocycle-closing, metathesis

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Publication details

The article was received on 19 Mar 2008, accepted on 20 Mar 2008 and first published on 10 Apr 2008


Article type: Communication
DOI: 10.1039/B804769N
Citation: Org. Biomol. Chem., 2008,6, 1734-1737
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    An efficient method for synthesising unsymmetrical silaketals: substrates for ring-closing, including macrocycle-closing, metathesis

    C. Cordier, D. Morton, S. Leach, T. Woodhall, C. O'Leary-Steele, S. Warriner and A. Nelson, Org. Biomol. Chem., 2008, 6, 1734
    DOI: 10.1039/B804769N

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