Issue 8, 2008
From the journal:

Green Chemistry

Microwave facile preparation of highly active and dispersed SBA-12 supported metal nanoparticles

Juan Manuel Campelo,a   Tomas David Conesa,a   Maria Jose Gracia,a   Maria Jose Jurado,a   Rafael Luque,*b   Jose Maria Marinasa  and  Antonio Angel Romeroa  

* Corresponding authors

a Departamento de Química Orgánica, Campus de Rabanales, Edificio Marie Curie, Ctra Nnal IV, Km 396, Universidad de Córdoba, Córdoba, Spain

b Green Chemistry Centre of Excellence, The University of York, Heslington, York, UK
E-mail: q62alsor@uco.es, rla3@york.ac.uk

Abstract

The successful preparation of highly active and dispersed metal nanoparticles on a mesoporous material was accomplished in a conventional microwave oven using an environmentally friendly protocol in which ethanol and acetone–water were employed as both solvents and reducing agents. The materials exhibited different particle sizes depending on the metal and the time of microwave irradiation. The nanoparticles were very active and differently selective in the oxidation of styrene.

Graphical abstract: Microwave facile preparation of highly active and dispersed SBA-12 supported metal nanoparticles

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Article information

DOI
https://doi.org/10.1039/B801754A
Article type
Paper
Submitted
31 Jan 2008
Accepted
09 May 2008
First published
23 Jun 2008

Green Chem., 2008,10, 853-858

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Microwave facile preparation of highly active and dispersed SBA-12 supported metal nanoparticles

J. M. Campelo, T. D. Conesa, M. J. Gracia, M. J. Jurado, R. Luque, J. M. Marinas and A. A. Romero, Green Chem., 2008, 10, 853 DOI: 10.1039/B801754A

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