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Issue 23, 2007
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Synthesis and reactivity of [18F]-N-fluorobenzenesulfonimide

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Abstract

A novel [18F]NF reagent and two novel radiochemical transformations have been developed: [18F]NFSi has been prepared from sodium dibenzenesulfonimide and reacted in the presence of silyl enol ethers and allylsilanes to deliver labelled fluorinated ketones and allylic fluorides respectively; the radiosynthesis of the fluorinated A ring of vitamin D3 has also been completed with success.

Graphical abstract: Synthesis and reactivity of [18F]-N-fluorobenzenesulfonimide

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Publication details

The article was received on 25 Jan 2007, accepted on 23 Feb 2007 and first published on 14 Mar 2007


Article type: Communication
DOI: 10.1039/B701177F
Citation: Chem. Commun., 2007,0, 2330-2332
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    Synthesis and reactivity of [18F]-N-fluorobenzenesulfonimide

    H. Teare, E. G. Robins, E. Årstad, S. K. Luthra and V. Gouverneur, Chem. Commun., 2007, 0, 2330
    DOI: 10.1039/B701177F

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