Benign approaches for the synthesis of bis-imine Schiff bases

Tania R. van den Ancker; Gareth W. V. Cave; Colin L. Raston

doi:10.1039/B513289D

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Green Chemistry

Issue 1, 2006

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Paper

Benign approaches for the synthesis of bis-imine Schiff bases

Tania R. van den Ancker,*^a Gareth W. V. Cave^b and Colin L. Raston^c

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Corresponding authors

Department of Biological and Physical Sciences, University of Southern Queensland, Toowoomba, Australia
E-mail: ancker@usq.edu.au ;
Fax: +61 7 4631 1530 ;
Tel: +61 7 4631 2363

School of Biomedical and Natural Sciences, Nottingham Trent University, Nottingham, UK
E-mail: gareth.cave@ntu.ac.uk ;
Fax: +44 (0)115 848 6636 ;
Tel: +44 (0)115 848 3242

School of Biomedical, Biomolecular and Chemical Sciences, University of Western Australia, Crawley, Australia
E-mail: clraston@chem.uwa.edu.au ;
Fax: +61 8 9380 1005 ;
Tel: +61 8 9380 3045

Green Chem., 2006,8, 50-53

DOI: 10.1039/B513289D
Received 22 Sep 2005, Accepted 28 Oct 2005
First published online 17 Nov 2005

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Pure bis-imine Schiff bases are readily accessible in high yield, typically >95%, when aliphatic diamine/aldehyde condensation reactions are carried out under solvent-free conditions or in poly(propyleneglycol) (PPG) as a recyclable reaction medium, with negligible waste.