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Issue 21, 2003
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Enhanced 13C resolution in semi-selective HMBC: a band-selective, constant-time HMBC for complex organic structure elucidation by NMR

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Abstract

A semi-selective 2D HMBC experiment is described which yields high-resolution in the indirect carbon-13 dimension by suppressing homonuclear proton coupling modulations and so provides an NMR technique suitable for the structure elucidation of organic compounds which exhibit particularly crowded carbon-13 spectra.

Graphical abstract: Enhanced 13C resolution in semi-selective HMBC: a band-selective, constant-time HMBC for complex organic structure elucidation by NMR

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Publication details

The article was received on 25 Jun 2003, accepted on 15 Jul 2003 and first published on 24 Jul 2003


Article type: Communication
DOI: 10.1039/B307122G
Citation: Org. Biomol. Chem., 2003,1, 3632-3634
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    Enhanced 13C resolution in semi-selective HMBC: a band-selective, constant-time HMBC for complex organic structure elucidation by NMR

    T. D. W. Claridge and I. Pérez-Victoria, Org. Biomol. Chem., 2003, 1, 3632
    DOI: 10.1039/B307122G

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