Issue 6, 2001

Abstract

A method for the simultaneous solvent extraction into IBMK from acidic medium of Cd(II), Cu(II), Co(II), Cr(VI), Ni(II), Pb(II) and Zn(II) as dibenzyldithiocarbamates and determination by AAS is proposed. Formal techniques for multidimensional optimization have been used, in particular, the response surface methodology, in order to obtain the best output variable to be optimized. The method was validated by applying it to some synthetic samples. In all cases, the trueness test indicated that the method was reliable, at least, for the samples analysed, which was confirmed by the recovery values obtained. The RSD values indicated a satisfactory precision.

Article information

Article type
Paper
Submitted
19 Feb 2001
Accepted
10 Apr 2001
First published
22 May 2001

J. Anal. At. Spectrom., 2001,16, 638-642

Multivariate optimization of solvent extraction of Cd(II), Co(II), Cr(VI), Cu(II), Ni(II), Pb(II) and Zn(II) as dibenzyldithiocarbamates and detection by AAS

M. Camino, M. G. Bagur, M. Sánchez-Viñas, D. Gázquez and R. Romero, J. Anal. At. Spectrom., 2001, 16, 638 DOI: 10.1039/B101590G

To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.

If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.

If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.

Read more about how to correctly acknowledge RSC content.

Social activity

Spotlight

Advertisements