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Issue 12, 1999
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A general and efficient procedure for the preparation of enantiopure anti-1,2-diols—synthesis and utility of (R<img border='0' src='http://www.rsc.org/images/entities/h2_char_200a.gif' alt=' '/>′,R<img border='0' src='http://www.rsc.org/images/entities/h2_char_200a.gif' alt=' '/>′,S,R)-2,3-butane diacetal protected butane tetrol

Abstract

The synthesis and utility of 2,3-butane diacetal protected butane tetrol (R ′,R ′,R,S )-2 for the general and efficient production of enantiopure anti-1,2-diols through selective silylation, alkylation and acetalisation of the spatially different hydroxy termini is described.

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Article type: Paper
DOI: 10.1039/A902732G
Citation: J. Chem. Soc., Perkin Trans. 1, 1999, 1635-1638
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    A general and efficient procedure for the preparation of enantiopure anti-1,2-diols—synthesis and utility of (R<img border='0' src='http://www.rsc.org/images/entities/h2_char_200a.gif' alt=' '/>′,R<img border='0' src='http://www.rsc.org/images/entities/h2_char_200a.gif' alt=' '/>′,S,R)-2,3-butane diacetal protected butane tetrol

    D. J. Dixon, A. C. Foster, S. V. Ley and D. J. Reynolds, J. Chem. Soc., Perkin Trans. 1, 1999, 1635
    DOI: 10.1039/A902732G

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