Combined Fourier-transform (FT) IR and X-ray absorption fine structure (XAFS) studies of NiBr2 isolated in a nitrogen matrix have shown that it is non-linear (125° FTIR, 145° XAFS), with the shortest Ni–Nmatrix interaction at 2.61 Å, compared to a linear geometry in a methane matrix.
N. A. Young, J. Chem. Soc., Dalton Trans., 1996, 249 DOI: 10.1039/DT9960000249
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