The main hydrolysis species of uranyl ions, [(UO2)2(OH)2]2+ and [(UO2)3(OH)5]+, were identified by 17O n.m.r. spectroscopy, signals being observed at 2.0 and 6.7 p.p.m. relative to the uranyl ion, respectively.
W. Jung, H. Tomiyasu and H. Fukutomi, J. Chem. Soc., Chem. Commun., 1987, 372 DOI: 10.1039/C39870000372
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