A significant ‘sliding’ of the C atoms towards the O atoms is observed on passing from isotropic to anisotropic refinement of the light atoms in conventional room temperature X-ray investigations on metal carbonyl clusters; differences in bond lengths are discussed with respect to results of neutron diffraction studies.
D. Braga and T. F. Koetzle, J. Chem. Soc., Chem. Commun., 1987, 144 DOI: 10.1039/C39870000144
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