Racemic gossypol has been resolved rapidly and efficiently by h.p.l.c. separation of diastereoisomeric adducts formed with the β-amino alcohol, L-phenylalaninol, on an achiral, reverse-phase C18 column.
D. S. Sampath and P. Balaram, J. Chem. Soc., Chem. Commun., 1986, 649 DOI: 10.1039/C39860000649
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