SCHEDULED MAINTENANCE
Michael-type additions of phenylsulphinylacetate esters to αβ-unsaturated ketones produce cyclohexane-1,3-dione derivatives, which, after thermal elimination of benzenesulphenic acid, give the corresponding 5-substituted resorcinols, such as olivetol. The scope of this entry into other aromatic systems, such as 3,5-disubstituted and 2,3,5-trisubstituted phenols and orsellinic acid has been explored.
A. A. Jaxa-Chamiec, P. G. Sammes and P. D. Kennewell, J. Chem. Soc., Perkin Trans. 1, 1980, 170 DOI: 10.1039/P19800000170
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