SCHEDULED MAINTENANCE
Addition of diphenylbromoborane to di-isopropylcarbamoyl-lithium at low temperature followed by warming to ambient, and passage through silica gives 5-(di-isopropyliminio)-2,2,4,4-tetraphenyl-2,4-diborata-1-oxa-3-oxoniacyclopentane (2).
A. S. Fletcher, W. E. Paget, K. Smith, K. Swaminathan, J. H. Beynon, R. P. Morgan, M. Bozorgzadeh and M. J. Haley, J. Chem. Soc., Chem. Commun., 1979, 347 DOI: 10.1039/C39790000347
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