The metallacyclopentane–olefin interchange reaction

Robert H. Grubbs; Akira Miyashita

doi:10.1039/C39770000864

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Journal of the Chemical Society, Chemical Communications

Issue 23, 1977

Journal of the Chemical Society, Chemical Communications was published between 1972 - 1995.

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The metallacyclopentane–olefin interchange reaction

Robert H. Grubbs and Akira Miyashita

J. Chem. Soc., Chem. Commun., 1977, 864-865

DOI: 10.1039/C39770000864

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Abstract
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Tris(triphenylphosphine)tetramethylenenickel(II) and biscyclopentadienyltetramethylenetitanium, prepared from the reaction of a 1,4-dilithiobutane and the transition metal dihalides react with olefins to produce substituted metallacyclopentanes; the stereochemistry and substitution pattern of the metallocycles formed from propene, octa-1,7-diene, and norbornadiene has been determined.

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The metallacyclopentane–olefin interchange reaction

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