Pyrolysis of trimethylborane at 475–520 °C yields Me2BCH2BMe2 and the carboranes C2H2(BMe)3 and C4H4(BMe)6; mass spectral evidence suggests also the formation of (MeBCH2)3 and (MeBCH2)4 and other less-volatile carboranes.
M. P. Brown, A. K. Holliday and G. M. Way, J. Chem. Soc., Chem. Commun., 1972, 850 DOI: 10.1039/C39720000850
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