Issue 21, 1970

Crystal structure of oxochlorobis-[1,2-bis(diphenylphosphino)ethane]-molybdenum(IV) trichloro(acetone)zincate:[MoOCl{Ph2P(CH2)2PPh2}2]+[ZnCl3,OC(CH3)2]

Abstract

A crystal structure analysis of a purple complex obtained on reduction of MoOCl3{Ph2P-(CH2)2PPh2} with zinc dust in tetrahydrofuran followed by recrystallization from acetone shows the crystals to be [MoOCl{Ph2P(CH2)2PPh2}2]+[ZnCl3,OC(CH3)2],OC-(CH3)2.

Article information

Article type
Paper

J. Chem. Soc. D, 1970, 1400-1401

Crystal structure of oxochlorobis-[1,2-bis(diphenylphosphino)ethane]-molybdenum(IV) trichloro(acetone)zincate:[MoOCl{Ph2P(CH2)2PPh2}2]+[ZnCl3,OC(CH3)2]

V. C. Adam, U. A. Gregory and B. T. Kilbourn, J. Chem. Soc. D, 1970, 1400 DOI: 10.1039/C29700001400

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