SCHEDULED MAINTENANCE
The first example of an all-carbon anionic [3,2]-sigmatropic rearrangement has been observed in the conversion of 9-(3-methylbut-2-enyl)-9-(lithiomethyl)-fluorene into 9-(2,2-dimethylbut-3-enyl)-9-lithiofluorene, the reaction being accompanied by a temperature-dependent dissociation–recombination process.
J. E. Baldwin and F. J. Urban, J. Chem. Soc. D, 1970, 165 DOI: 10.1039/C29700000165
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