Issue 6, 2002
From the journal:

Journal of the Chemical Society, Perkin Transactions 1

Reactions of acyl chlorides with LiAlHSeH. Preparation of diacyl selenides, diacyl diselenides, selenocarboxylates and cyclic selenoanhydrides

Mamoru Koketsu,*a   Futoshi Nada,a   Sohma Hiramatsua  and  Hideharu Ishihara*a  

* Corresponding authors

a Department of Chemistry, Faculty of Engineering, Gifu University, Gifu 501-1193, Japan
E-mail: koketsu@cc.gifu-u.ac.jp
Fax: +81-58-230-1893

Abstract

Various diacyl selenides, diacyl diselenides and selenocarboxylates were synthesized by reaction of several acyl chlorides with LiAlHSeH. Reaction of diacyl chloride with LiAlHSeH afforded cyclic selenoanhydrides. In the 77Se NMR spectra, we found that the chemical shifts of the diacyl selenides and the diacyl diselenides could facilitate their distinction.

Graphical abstract: Reactions of acyl chlorides with LiAlHSeH. Preparation of diacyl selenides, diacyl diselenides, selenocarboxylates and cyclic selenoanhydrides

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Article information

DOI
https://doi.org/10.1039/B200147K
Article type
Paper
Submitted
08 Jan 2002
Accepted
08 Feb 2002
First published
22 Feb 2002

J. Chem. Soc., Perkin Trans. 1, 2002, 737-740

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Reactions of acyl chlorides with LiAlHSeH. Preparation of diacyl selenides, diacyl diselenides, selenocarboxylates and cyclic selenoanhydrides

M. Koketsu, F. Nada, S. Hiramatsu and H. Ishihara, J. Chem. Soc., Perkin Trans. 1, 2002, 737 DOI: 10.1039/B200147K

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