Issue 3, 2013

Rapid and efficient solvent-free synthesis of cyclophanes based on bipyridinium under mechanical ball milling

Abstract

We reported here the first rapid and solvent-free template-directed preparation of cyclophanes based on bipyridinium, which was achieved using mechanical ball milling. The method affords a new strategy for construction of diverse substituted CBPQT·4PF6, which greatly shortens the reaction period, rendering this methodology practical in the field of supermolecular chemistry.

Graphical abstract: Rapid and efficient solvent-free synthesis of cyclophanes based on bipyridinium under mechanical ball milling

Supplementary files

Article information

Article type
Communication
Submitted
07 Nov 2012
Accepted
08 Nov 2012
First published
08 Nov 2012

RSC Adv., 2013,3, 691-694

Rapid and efficient solvent-free synthesis of cyclophanes based on bipyridinium under mechanical ball milling

H. Xi, T. Zhao, X. Sun, C. Miao, T. Zong and Q. Meng, RSC Adv., 2013, 3, 691 DOI: 10.1039/C2RA22802E

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