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The structure of conocephalenol, a brasilane sesquiterpenoid alcohol isolated from the European liverwort Conocephalum conicum, has been determined by extensive NMR studies including a 2D INADEQUATE experiment and by total synthesis, which established the absolute stereochemistry as 1R,9S.
M. Tori, K. Nakashima, Y. Asakawa, J. D. Connolly, L. J. Harrison, D. S. Rycroft, J. Singh and N. Woods, J. Chem. Soc., Perkin Trans. 1, 1995, 593 DOI: 10.1039/P19950000593
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