The tertiary alcohol 5 has been resolved to 90% ee (42% yield) by hydrolysis of its oxalate 6b with porcine pancreatic lipase in pH 7 buffer containing 13%tert-butyl alcohol.
I. Brackenridge, R. McCague, S. M. Roberts and N. J. Turner, J. Chem. Soc., Perkin Trans. 1, 1993, 1093 DOI: 10.1039/P19930001093
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