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Issue 8, 2013
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Direct arylation of phenanthroline derivatives via oxidative C–H/C–H cross-coupling: synthesis and discovery of excellent ligands

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Abstract

A concise synthetic protocol for aryl functionalized phenanthrolines has been developed. It was demonstrated that 3,8-diphenyl-1,10-phenanthroline (7a) is competent in promoting transition-metal-free direct arylation and 2,3,8,9-tetraphenyl-1,10-phenanthroline (8a) is a highly efficient ligand in the in situ Pd-catalysed Heck reaction.

Graphical abstract: Direct arylation of phenanthroline derivatives via oxidative C–H/C–H cross-coupling: synthesis and discovery of excellent ligands

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Publication details

The article was received on 30 Nov 2012, accepted on 19 Dec 2012 and first published on 20 Dec 2012


Article type: Communication
DOI: 10.1039/C2OB27325J
Citation: Org. Biomol. Chem., 2013,11, 1290-1293
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    Direct arylation of phenanthroline derivatives via oxidative C–H/C–H cross-coupling: synthesis and discovery of excellent ligands

    B. Li, X. Qin, J. You, X. Cong and J. Lan, Org. Biomol. Chem., 2013, 11, 1290
    DOI: 10.1039/C2OB27325J

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