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Issue 14, 2012
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One-pot sequential Ti-/Cu-catalysis for tandem amidation/Ullmann-type cyclization: synthesis of model benzodiazepine(di)ones promoted by microwave irradiation

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Abstract

The application of sequential Ti-/Cu-catalysis in the model one-pot synthesis of benzodiazepine(di)ones promoted by microwave irradiation demonstrates the expediency of dual catalysis in coupling-cyclization methods useful for diversity-oriented synthesis.

Graphical abstract: One-pot sequential Ti-/Cu-catalysis for tandem amidation/Ullmann-type cyclization: synthesis of model benzodiazepine(di)ones promoted by microwave irradiation

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Publication details

The article was received on 09 Dec 2011, accepted on 30 Jan 2012 and first published on 31 Jan 2012


Article type: Paper
DOI: 10.1039/C2OB07063D
Citation: Org. Biomol. Chem., 2012,10, 2780-2786
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    One-pot sequential Ti-/Cu-catalysis for tandem amidation/Ullmann-type cyclization: synthesis of model benzodiazepine(di)ones promoted by microwave irradiation

    L. Ciofi, A. Trabocchi, C. Lalli, G. Menchi and A. Guarna, Org. Biomol. Chem., 2012, 10, 2780
    DOI: 10.1039/C2OB07063D

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