Issue 4, 2012
From the journal:

Green Chemistry

Microwave-assisted synthesis of 2,3-dihydropyrido[2,3-d]pyrimidin-4(1H)-ones catalyzed by DBU in aqueous medium†

Liupan Yang,a   Daxin Shi,a   Shu Chen,a   Hongxin Chai,a   Danfei Huang,a   Qi Zhanga  and  Jiarong Li*a  

* Corresponding authors

a School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing, China
E-mail: jrli@bit.edu.cn
Fax: +86(10)68918012

Abstract

A clean green, efficient and facile protocol was developed for the synthesis of a series of 2,3-dihydropyrido[2,3-d]pyrimidin-4(1H)-ones in water with good yield by the reaction of 2-amino-nicotinonitriles with carbonyls catalyzed by DBU under microwave irradiation. The DBU–H2O system can be recycled five times without activity loss.

Graphical abstract: Microwave-assisted synthesis of 2,3-dihydropyrido[2,3-d]pyrimidin-4(1H)-ones catalyzed by DBU in aqueous medium

About
Cited by
Related
Download options Please wait...

Supplementary files

Article information

DOI
https://doi.org/10.1039/C2GC16469H
Article type
Paper
Submitted
17 Nov 2011
Accepted
04 Jan 2012
First published
10 Feb 2012

Green Chem., 2012,14, 945-951

Permissions

Request permissions

Microwave-assisted synthesis of 2,3-dihydropyrido[2,3-d]pyrimidin-4(1H)-ones catalyzed by DBU in aqueous medium

L. Yang, D. Shi, S. Chen, H. Chai, D. Huang, Q. Zhang and J. Li, Green Chem., 2012, 14, 945 DOI: 10.1039/C2GC16469H

To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.

If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.

If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.

Read more about how to correctly acknowledge RSC content.

Social activity

Spotlight

Advertisements