Issue 9, 2008
From the journal:

Green Chemistry

Rapid and convenient laboratory method for the preparation of p-tert-butylcalix[4]arene using microwave irradiation

Masafumi Takagaki,a   Asao Hosoda,a   Hajime Mori,a   Yasuhito Miyake,a   Keiichi Kimura,b   Hisaji Taniguchia  and  Eisaku Nomura*c  

* Corresponding authors

a Industrial Technology Centre of Wakayama Prefecture, 60 Ogura, Wakayama, Japan

b Faculty of Material Science, Wakayama University, 930 Sakaedani, Wakayama, Japan

c Department of Material Science, Wakayama National College of Technology, 77 Noshima, Nada, Gobo Wakayama, Japan
E-mail: nomura@wakayama-nct.ac.jp
Fax: +81-738-29-8439
Tel: +81-738-23-8415

Abstract

Rapid preparation of p-tert-butylcalix[4]arene using microwave irradiation was studied and p-tert-butylcalix[4]arene was obtained as a pure form in modest yield with shortening the reaction time from hours to minutes.

Graphical abstract: Rapid and convenient laboratory method for the preparation of p-tert-butylcalix[4]arene using microwave irradiation

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Article information

DOI
https://doi.org/10.1039/B801715H
Article type
Paper
Submitted
30 Jan 2008
Accepted
18 Jun 2008
First published
08 Aug 2008

Green Chem., 2008,10, 978-981

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Rapid and convenient laboratory method for the preparation of p-tert-butylcalix[4]arene using microwave irradiation

M. Takagaki, A. Hosoda, H. Mori, Y. Miyake, K. Kimura, H. Taniguchi and E. Nomura, Green Chem., 2008, 10, 978 DOI: 10.1039/B801715H

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