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Issue 24, 2012
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A novel hydrate of α-cyclodextrin crystallised under high-pressure conditions

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Abstract

The technique of high-pressure crystallisation from solution has been applied to the study of α-cyclodextrin hydrate formation. A previously unobserved hydrate, here termed Ib, has been obtained at 0.65 GPa and characterised by single-crystal X-ray diffraction using synchrotron radiation. This form exhibits a combination of structural features of other known hydrates and hydration states obtained by theoretical calculations but never found experimentally before.

Graphical abstract: A novel hydrate of α-cyclodextrin crystallised under high-pressure conditions

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Publication details

The article was received on 23 Aug 2012, accepted on 03 Oct 2012 and first published on 18 Oct 2012


Article type: Paper
DOI: 10.1039/C2CE26362A
Citation: CrystEngComm, 2012,14, 8664-8670
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    A novel hydrate of α-cyclodextrin crystallised under high-pressure conditions

    R. Granero-García, F. J. Lahoz, C. Paulmann, S. Saouane and F. P. A. Fabbiani, CrystEngComm, 2012, 14, 8664
    DOI: 10.1039/C2CE26362A

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