A novel porous chiral In-MOF InH(D-C10H14O4)2 (1) with a left-handed helical channel assembled from D-(+)-camphoric acid (D-H2Cam), has been prepared under solvothermal conditions. Single-crystal X-ray diffraction analysis reveals that compound 1 crystallizes in the tetragonal space group P43212 (no. 96) with parameters: a = 13.8954 Å, b = 13.8954 Å, c = 17.7870 Å, V = 3434.4(7) Å 3, Z = 4. The framework feature of compound 1 is characteristic of four-connected anionic-type diamond net with left-handed chiral channel. Moreover, compound 1 exhibits high surface area.
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