Issue 80, 2017

Silicon diimide gel as an efficient stationary phase in thin layer chromatography for acid-sensitive organic compounds

Abstract

We report the use of mesoporous silicon diimide gel as a basic stationary phase in thin layer chromatography for the characterisation and purification of acid-sensitive compounds. The gel is prepared by a simple sol–gel process and exhibits a large specific surface area, almost monodisperse pores and basic properties due to free-hanging amine groups.

Graphical abstract: Silicon diimide gel as an efficient stationary phase in thin layer chromatography for acid-sensitive organic compounds

Article information

Article type
Communication
Submitted
26 Jun 2017
Accepted
19 Sep 2017
First published
19 Sep 2017

Chem. Commun., 2017,53, 11080-11082

Silicon diimide gel as an efficient stationary phase in thin layer chromatography for acid-sensitive organic compounds

S. P. Kitney, S. M. Sajedin, V. Rocher, F. Cheng and S. M. Kelly, Chem. Commun., 2017, 53, 11080 DOI: 10.1039/C7CC04952H

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