Issue 31, 2016
From the journal:

Chemical Communications

Cu-catalyzed C–H amination/Ullmann N-arylation domino reaction: a straightforward synthesis of 9,14-diaryl-9,14-dihydrodibenzo[a,c]phenazine†

Huan Wang,a   Zhiyun Zhang,a   Haitao Zhou,a   Tonghai Wang,a   Jianhua Su,*a   Xiaofeng Tong*a  and  He Tiana  

* Corresponding authors

a Key Laboratory for Advanced Materials and Institute of Fine Chemicals, East China University of Science and Technology, 130 Meilong Road, Shanghai 200237, China
E-mail: bbsjh@ecust.edu.cn, txf@cczu.edu.cn

Abstract

A Cu-catalyzed C–H amination/Ullmann N-arylation domino reaction of phenanthrene-9,10-diamines with aryl iodides has been developed, which provides a straightforward and facile access to 9,14-diaryl-9,14-dihydrodibenzo[a,c]phenazine. This reaction features readily available starting materials and simple experimental operation.

Graphical abstract: Cu-catalyzed C–H amination/Ullmann N-arylation domino reaction: a straightforward synthesis of 9,14-diaryl-9,14-dihydrodibenzo[a,c]phenazine

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Article information

DOI
https://doi.org/10.1039/C6CC01569G
Article type
Communication
Submitted
21 Feb 2016
Accepted
16 Mar 2016
First published
16 Mar 2016

Chem. Commun., 2016,52, 5459-5462

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Cu-catalyzed C–H amination/Ullmann N-arylation domino reaction: a straightforward synthesis of 9,14-diaryl-9,14-dihydrodibenzo[a,c]phenazine

H. Wang, Z. Zhang, H. Zhou, T. Wang, J. Su, X. Tong and H. Tian, Chem. Commun., 2016, 52, 5459 DOI: 10.1039/C6CC01569G

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