Use of in situneutron diffraction to monitor high-temperature, solid/H2-gas reactions

Florent Tonus; Mona Bahout; Paul F. Henry; Siân E. Dutton; Thierry Roisnel; Peter D. Battle

doi:10.1039/B822419F

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Use of in situneutron diffraction to monitor high-temperature, solid/H₂-gas reactions†

Florent Tonus,^a Mona Bahout,*^a Paul F. Henry,‡^b Siân E. Dutton,^c Thierry Roisnel^a and Peter D. Battle*^c

Author affiliations

* Corresponding authors

^a Université de Rennes 1, Laboratoire Sciences Chimiques de Rennes, UMR CNRS 6226, 263 avenue du général Leclerc, Rennes CEDEX, France
E-mail: Mona.Bahout@univ-rennes1.fr
Fax: +33 223236799
Tel: +33 223236981

^b Institut Laue Langevin, 6 Rue Jules Horowitz, BP156, Grenoble CEDEX 9, France

^c Inorganic Chemistry Laboratory, Oxford University, South Parks Road, Oxford, UK
E-mail: peter.battle@chem.ox.ac.uk
Fax: + 44 (0)1865 272690
Tel: +44 (0)1865 272612

Abstract

For the first time, the chemistry in H₂ gas of a perovskite-like material, Pr₂Sr₂CrNiO₈, has been monitored at temperatures up to ∼700 °C, in situ, by neutron powder diffraction.

$Graphical abstract: Use of in situneutron diffraction to monitor high-temperature, solid/H2-gas reactions$

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Supplementary files

Fitted neutron diffraction patterns and structuralparameters PDF (355K)

Article information

DOI: https://doi.org/10.1039/B822419F
Article type: Communication
Submitted: 15 Dec 2008
Accepted: 23 Feb 2009
First published: 17 Mar 2009

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Chem. Commun., 2009, 2556-2558

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Use of in situneutron diffraction to monitor high-temperature, solid/H₂-gas reactions

F. Tonus, M. Bahout, P. F. Henry, S. E. Dutton, T. Roisnel and P. D. Battle, Chem. Commun., 2009, 2556 DOI: 10.1039/B822419F

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