Issue 23, 2007
From the journal:

Chemical Communications

Copper-catalyzed oxidative desulfurization–oxygenation of thiocarbonyl compounds using molecular oxygen: an efficient method for the preparation of oxygen isotopically labeled carbonyl compounds†

Fumitoshi Shibahara,*a   Aiko Suenami,a   Atsunori Yoshidaa  and  Toshiaki Murai*a  

* Corresponding authors

a Department of Chemistry, Faculty of Engineering, Gifu University, Yanagido, Gifu, Japan
E-mail: fshiba@gifu-u.ac.jp, mtoshi@gifu-u.ac.jp
Fax: +81 58 230 1893
Tel: +81 58 293 2616

Abstract

A novel copper-catalyzed oxidative desulfurization reaction of thiocarbonyl compounds, using molecular oxygen as an oxidant and leading to formation of carbonyl compounds, has been developed, and the utility of the process is demonstrated by its application to the preparation of a carbonyl-18O labeled sialic acid derivative.

Graphical abstract: Copper-catalyzed oxidative desulfurization–oxygenation of thiocarbonyl compounds using molecular oxygen: an efficient method for the preparation of oxygen isotopically labeled carbonyl compounds

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Article information

DOI
https://doi.org/10.1039/B701048F
Article type
Communication
Submitted
23 Jan 2007
Accepted
14 Feb 2007
First published
08 Mar 2007

Chem. Commun., 2007, 2354-2356

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Copper-catalyzed oxidative desulfurization–oxygenation of thiocarbonyl compounds using molecular oxygen: an efficient method for the preparation of oxygen isotopically labeled carbonyl compounds

F. Shibahara, A. Suenami, A. Yoshida and T. Murai, Chem. Commun., 2007, 2354 DOI: 10.1039/B701048F

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