Issue 7, 2004
From the journal:

Chemical Communications

Detecting proximities between quadrupolar nuclei by double-quantum NMR

Gregor Mali*a  and  Francis Taulelleb  

* Corresponding authors

a National Institute of Chemistry, Hajdrihova 19, SI-1001 Ljubljana, Slovenia
E-mail: gregor.mali@ki.si

b RMN et Chimie du Solide, Tectonique Moleculaire du Solide, UMR CNRS 7140, Universite Louis Pasteur, 4 Rue Blaise Pascal, F-67070 Strasbourg cedex, France
E-mail: taulelle@chimie.u-strasbg.fr

Abstract

A robust, easy to optimize, and efficient homonuclear correlation NMR experiment for half-integer quadrupolar nuclei in solids is described and has been experimentally tested on anhydrous Na2HPO4 (23Na, S = 3/2 nucleus) and as-synthesized AlPO4-14 (27Al, S = 5/2 nucleus), an aluminophosphate molecular sieve.

Graphical abstract: Detecting proximities between quadrupolar nuclei by double-quantum NMR

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Article information

DOI
https://doi.org/10.1039/B316807G
Article type
Communication
Submitted
05 Jan 2004
Accepted
06 Feb 2004
First published
27 Feb 2004

Chem. Commun., 2004, 868-869

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Detecting proximities between quadrupolar nuclei by double-quantum NMR

G. Mali and F. Taulelle, Chem. Commun., 2004, 868 DOI: 10.1039/B316807G

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