First observation of high-resolution solid-state 73Ge NMR spectra of organogermanium compounds

Yoshito Takeuchi; Miki Nishikawa; Katsumi Tanaka; Toshio Takayama; Mamoru Imanari; Kenzou Deguchi; Teruaki Fujito; Yasushi Sugisaka

doi:10.1039/B001011L

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First observation of high-resolution solid-state ⁷³Ge NMR spectra of organogermanium compounds

Yoshito Takeuchi,*^a Miki Nishikawa,^a Katsumi Tanaka,^a Toshio Takayama,^b Mamoru Imanari,^c Kenzou Deguchi,^c Teruaki Fujito^c and Yasushi Sugisaka^c

Author affiliations

* Corresponding authors

^a Department of Chemistry, Faculty of Science, Kanagawa University, 2946 Tsuchiya, Hiratsuka-shi, Japan
E-mail: yoshito@info.kanagawa-u.ac.jp

^b Department of Applied Chemistry, Faculty of Engineering, Kanagawa University, 3-27-1 Rokkakubashi, Kanagawa-ku, Yokohama-shi, Japan

^c NMR Application Laboratory, JEOL Ltd., 3-1-2 Musashino, Akishima-shi, Tokyo, Japan

Abstract

High-resolution solid-state MAS ⁷³Ge NMR spectra of organogermanium compounds have been observed for the first time; the chemical shifts and half-widths of tetraphenylgermane and tetrabenzylgermane were recorded with and without high-power decoupling.

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Article information

DOI: https://doi.org/10.1039/B001011L
Article type: Communication
Submitted: 07 Feb 2000
Accepted: 15 Mar 2000
First published: 30 Mar 2000

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Chem. Commun., 2000, 687-688

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First observation of high-resolution solid-state ⁷³Ge NMR spectra of organogermanium compounds

Y. Takeuchi, M. Nishikawa, K. Tanaka, T. Takayama, M. Imanari, K. Deguchi, T. Fujito and Y. Sugisaka, Chem. Commun., 2000, 687 DOI: 10.1039/B001011L

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Chemical Communications

First observation of high-resolution solid-state ⁷³Ge NMR spectra of organogermanium compounds

Abstract

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First observation of high-resolution solid-state ⁷³Ge NMR spectra of organogermanium compounds

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