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The IJKLM ring fragment of CTX3C, an important member of the ciguatoxin family, was synthesized via ring-closing metathesis using the Tebbe reagent and an improved method of reductive hydroxy ketone cyclization.
T. Oishi, Y. Nagumo, M. Shoji, J. Le Brazidec, H. Uehara and M. Hirama, Chem. Commun., 1999, 2035 DOI: 10.1039/A906834A
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