The two-steps synthesis of C-glycosyl juglones, versatile synthetic intermediates for angucycline antibiotics, has been developed by the C-glycosidation of naphthalene-1,5-diol with an unprotected sugar and the subsequent regioselective photooxygenation of the resultant C-glycosyl naphthalenediol.
G. Matsuo, S. Matsumura and K. Toshima, Chem. Commun., 1996, 2173 DOI: 10.1039/CC9960002173
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