SCHEDULED MAINTENANCE
Generation of a phosphonyl radical either from diethyl phosphite, or diethyl (phenylselenyl)phosphonate in conjunction with tributylstannane, in the presence of a carbohydrate gem-difluoroenol ether provides a new route to anomeric difluoromethylenephosphonates; in the course of these reactions, some unusual stereochemical effects are observed.
T. F. Herpin, J. S. Houlton, W. B. Motherwell, B. P. Roberts and J. Weibel, Chem. Commun., 1996, 613 DOI: 10.1039/CC9960000613
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