SCHEDULED MAINTENANCE
The alkaloid melinonine-E has been synthesised for the first time, the key steps being the elaboration of the 2-azabicyclo[3.3.l]nonane nucleus by a radical cyclisation, the epimerisation of the cyano group to an axial position, and the closure of the C ring by Bischler–Napieralski cyclisation.
J. Quirante, C. Escolano, J. Bosch and J. Bonjoch, J. Chem. Soc., Chem. Commun., 1995, 2141 DOI: 10.1039/C39950002141
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