Complexes [Mo3X12]3–(X = I, Br) assemble by spontaneous thf loss in noncoordinating solvents from [MoX4(thf)2]– and exhibit a linear face-shared trioctahedral structure with, at the same time, delocalized metal–metal bonding and local moment antiferromagnetic exchange interactions.
J. C. Fettinger, S. P. Mattamana, C. J. O'Connor, R. Poli and G. Salem, J. Chem. Soc., Chem. Commun., 1995, 1265 DOI: 10.1039/C39950001265
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