Reaction of [NH4]2[MoS4], CuCN and [Bun4N]Br in the solid state produced the mixed-metal sulphur cluster anion [Cu12Mo8S32]4–; an X-ray analysis of [Bun4N]4[Cu12Mo8S32] shows that the anion forms a cubane-like [Cu12Mo8] bimetallic cage through µ1-S, µ2-S, µ3-S and µ4-S atoms.
L. Jiguo, X. Xinquan, Z. Zhongyuan and Y. Kaibei, J. Chem. Soc., Chem. Commun., 1991, 249 DOI: 10.1039/C39910000249
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