Reaction of benzene with sodium/potassium alloy and dichloro(di-isopropylamino)borane (1 : 2) in 1,2-dimethoxyethane gives, in addition to other products, the title compound, characterised by its mass (El, Fl) and NMR (1H, 11B, 13C) spectra and X-ray crystallography.
A. Meller, D. Bromm, W. Maringgele, A. Heine, D. Stalke and G. M. Sheldrick, J. Chem. Soc., Chem. Commun., 1990, 741 DOI: 10.1039/C39900000741
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