SCHEDULED MAINTENANCE
Pertrimethylsilylation of N-acetylamphotericin B methyl ester (2) using trimethylsilyl trifluoromethanesulphonate results in anomeric elimination to give the 13,14-anhydro derivative (5) rather than the reported 13-O-trimethylsilyl ether (3).
M. J. Driver, W. S. MacLachlan, D. T. MacPherson and S. A. Readshaw, J. Chem. Soc., Chem. Commun., 1990, 636 DOI: 10.1039/C39900000636
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