Reaction of SbCl5 with graphite at room temperature results in the formation of a dilute first-stage intercalate consisting of several species, including SbCl3, Sbcl52–, SbCl6– and SbCl63–; the occurrence of an unusual low-temperature phase transition is also discussed.
W. Jones, P. Korgul, R. Schlögl and J. M. Thomas, J. Chem. Soc., Chem. Commun., 1983, 468 DOI: 10.1039/C39830000468
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