We quantitatively analysed when the chirality enrichment proceeded during temperature cycle-induced deracemization by monitoring crystalline ee during a single heating-cooling cycle. The enrichment proceeded during dissolution steps. Furthermore, evolution and devolution of ee could be described by mass and surface area ratio between the enantiomeric crystals.
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R. Oketani, R. Naito and I. Hisaki, Chem. Commun., 2026, Accepted Manuscript , DOI: 10.1039/D5CC04955E
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