A case study of Pd⋯Pd intramolecular interaction in a benzothiazole based palladacycle; catalytic activity toward amide synthesis via an isocyanide insertion pathway

Masood Loni; Yaser Balmohammadi; Reza Dadgar Yeganeh; Kaveh Imani; Behrouz Notash; Ayoob Bazgir

doi:10.1039/D0NJ06301K

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A case study of Pd⋯Pd intramolecular interaction in a benzothiazole based palladacycle; catalytic activity toward amide synthesis via an isocyanide insertion pathway†

Masood Loni,^a Yaser Balmohammadi,^a Reza Dadgar Yeganeh,^a Kaveh Imani,^a Behrouz Notash^b and Ayoob Bazgir

*^a

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* Corresponding authors

^a Department of Chemistry, Shahid Beheshti University, Tehran 1983963113, Iran
E-mail: a_bazgir@sbu.ac.ir

^b Department of Inorganic Chemistry and Catalysis, Shahid Beheshti University, Evin, Tehran, Iran

Abstract

An acetate bridge benzothiazolepalladacycle containing a rare metallophilic intramolecular Pd⋯Pd interaction was synthesized and thoroughly characterized. The synthesized benzothiazolepalladacycle directly anchored on SBA-15 to form an efficient heterogeneous catalyst for amide synthesis via the migratory isocyanide insertion pathway.

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DOI: https://doi.org/10.1039/D0NJ06301K
Article type: Paper
Submitted: 29 Dec 2020
Accepted: 19 Jan 2021
First published: 20 Jan 2021

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New J. Chem., 2021,45, 3290-3297

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A case study of Pd⋯Pd intramolecular interaction in a benzothiazole based palladacycle; catalytic activity toward amide synthesis via an isocyanide insertion pathway

M. Loni, Y. Balmohammadi, R. Dadgar Yeganeh, K. Imani, B. Notash and A. Bazgir, New J. Chem., 2021, 45, 3290 DOI: 10.1039/D0NJ06301K

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New Journal of Chemistry

A case study of Pd⋯Pd intramolecular interaction in a benzothiazole based palladacycle; catalytic activity toward amide synthesis via an isocyanide insertion pathway†

Abstract

Supplementary files

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A case study of Pd⋯Pd intramolecular interaction in a benzothiazole based palladacycle; catalytic activity toward amide synthesis via an isocyanide insertion pathway

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