Metal-free synthesis of imino-disaccharides and calix-iminosugars by photoinduced radical thiol–ene coupling (TEC)

Renaud Zelli; Pascal Dumy; Alberto Marra

doi:10.1039/D0OB00198H

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Metal-free synthesis of imino-disaccharides and calix-iminosugars by photoinduced radical thiol–ene coupling (TEC)†

Renaud Zelli,^a Pascal Dumy

^a and Alberto Marra

*^a

Author affiliations

* Corresponding authors

^a Institut des Biomolécules Max Mousseron (IBMM), UMR 5247, CNRS, Université de Montpellier, Ecole Nationale Supérieure de Chimie de Montpellier, 8 Rue de l'Ecole Normale, 34296 Montpellier cedex 5, France
E-mail: Alberto.Marra@umontpellier.fr

Abstract

Radical thiol–ene coupling was exploited for the first time to prepare imino-disaccharides and multivalent iminosugars starting from sugar thiols and iminosugar alkenes or iminosugar thiols and tetra-allylated calixarene, respectively.

This article is part of the themed collections: Chemical Biology in OBC and Synthetic methodology in OBC

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Article information

DOI: https://doi.org/10.1039/D0OB00198H
Article type: Communication
Submitted: 30 Jan 2020
Accepted: 13 Feb 2020
First published: 21 Feb 2020

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Org. Biomol. Chem., 2020,18, 2392-2397

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Metal-free synthesis of imino-disaccharides and calix-iminosugars by photoinduced radical thiol–ene coupling (TEC)

R. Zelli, P. Dumy and A. Marra, Org. Biomol. Chem., 2020, 18, 2392 DOI: 10.1039/D0OB00198H

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Organic & Biomolecular Chemistry

Metal-free synthesis of imino-disaccharides and calix-iminosugars by photoinduced radical thiol–ene coupling (TEC)†

Abstract

Supplementary files

Article information

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Metal-free synthesis of imino-disaccharides and calix-iminosugars by photoinduced radical thiol–ene coupling (TEC)

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