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Pushing the limits of sensitivity and resolution for natural abundance 43Ca NMR using ultra-high magnetic field (35.2 T)

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Abstract

Natural abundance 43Ca solid state NMR experiments are reported for the first time at ultra-high magnetic field (35.2 T) on a series of Ca-(pyro)phosphate and Ca-oxalate materials, which are of biological relevance in relation to biomineralization processes and the formation of pathological calcifications. The significant gain in both sensitivity and resolution at 35.2 T leads to unprecedented insight into the structure of both crystalline and amorphous phases.

Graphical abstract: Pushing the limits of sensitivity and resolution for natural abundance 43Ca NMR using ultra-high magnetic field (35.2 T)

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Publication details

The article was received on 28 Jun 2018, accepted on 02 Aug 2018 and first published on 02 Aug 2018


Article type: Communication
DOI: 10.1039/C8CC05193C
Citation: Chem. Commun., 2018, Advance Article
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    Pushing the limits of sensitivity and resolution for natural abundance 43Ca NMR using ultra-high magnetic field (35.2 T)

    C. Bonhomme, X. Wang, I. Hung, Z. Gan, C. Gervais, C. Sassoye, J. Rimsza, J. Du, M. E. Smith, J. V. Hanna, S. Sarda, P. Gras, C. Combes and D. Laurencin, Chem. Commun., 2018, Advance Article , DOI: 10.1039/C8CC05193C

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