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Issue 65, 2018
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Rapid access to RNA resonances by proton-detected solid-state NMR at >100 kHz MAS

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Abstract

Fast (>100 kHz) magic angle spinning solid-state NMR allows combining high-sensitive proton detection with the absence of an intrinsic molecular weight limit. Using this technique we observe for the first time narrow 1H RNA resonances and assign nucleotide spin systems with only 200 μg of uniformly 13C,15N-labelled RNA.

Graphical abstract: Rapid access to RNA resonances by proton-detected solid-state NMR at >100 kHz MAS

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Publication details

The article was received on 05 Jun 2018, accepted on 28 Jun 2018 and first published on 28 Jun 2018


Article type: Communication
DOI: 10.1039/C8CC04437F
Citation: Chem. Commun., 2018,54, 8972-8975
  • Open access: Creative Commons BY-NC license
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    Rapid access to RNA resonances by proton-detected solid-state NMR at >100 kHz MAS

    A. Marchanka, J. Stanek, G. Pintacuda and T. Carlomagno, Chem. Commun., 2018, 54, 8972
    DOI: 10.1039/C8CC04437F

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