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Real-time mass-spectrometric screening of droplet-scale electrochemical reactions

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Abstract

A droplet-scale, real-time electrochemical reaction screening platform based on droplet spray ionization mass spectrometry (DSI-MS) has been developed. The N,N-dimethylaniline (DMA) radical cation with a half-life of microseconds was readily detected by MS during the electrooxidation of DMA, and the subsequent reactions were followed in real time for minutes.

Graphical abstract: Real-time mass-spectrometric screening of droplet-scale electrochemical reactions

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Publication details

The article was received on 24 May 2018, accepted on 13 Jul 2018 and first published on 14 Jul 2018


Article type: Communication
DOI: 10.1039/C8AN00957K
Citation: Analyst, 2018, Advance Article
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    Real-time mass-spectrometric screening of droplet-scale electrochemical reactions

    H. Zhang, K. Yu, N. Li, J. He, L. Qiao, M. Li, Y. Wang, D. Zhang, J. Jiang and R. N. Zare, Analyst, 2018, Advance Article , DOI: 10.1039/C8AN00957K

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