A combination of UV-Vis spectroscopy and electrospray ionization mass spectrometry is used for real-time monitoring of Pd2(dba)3 activation with sulfonated versions of PPh3 and Buchwald-type ligands. This provides insight into the effect of ligand and preparation conditions on activation and allows for establishment of rational activation protocols.
E. Janusson, H. S. Zijlstra, P. P. T. Nguyen, L. MacGillivray, J. Martelino and J. S. McIndoe, Chem. Commun., 2017, 53, 854 DOI: 10.1039/C6CC08824D
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